![]() Insert the 3% CHCl3 in acetone-d6 sample. Once the issue has been identified, additional troubleshooting of sensitivity and/or lineshape can proceed. We ask that any time you have a question about lineshape or sensitivity, you first run one of the test protocols listed below in order to ensure that the issue is not related to your sample. Additional nuclei can be tested upon request. It also contains a recent set of lineshape and sensitivity spectra for 1H and 13C for reference. This page contains information regarding the Production specifications and the Installed specifications for the Varian/Agilent MR400. Typically, the two parameters of concern in NMR are resolution/lineshape and sensitivity. More detailed information about the proper instrument set-up and operational parameters necessary to reproduce these measurements can be found in the appropriate training manual or application note. A brief description of the acquisition protocol is given for each set of measurements. This page contains spectra that are representative of the normal level of performance of this instrument. ![]()
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